Spectroscopic identifications of structure II hydrate with new large alcohol guest molecule (Cyclopentanemethanol)

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초록

Herein the guest inclusions and interactions in a binary (cyclopentanemethanol + CH4) hydrate were explored via 13C NMR spectroscopy and XRD analysis. The 13C NMR spectra of the binary (cyclopentanemethanol + CH4) hydrate confirmed the formation of structure II hydrate with the inclusion of cyclopentanemethanol and CH4 in the structure II hydrate cages. Rietveld analysis on XRD profiles of the binary (cyclopentanemethanol + CH4) hydrate confirmed the formation of a cubic Fd3m hydrate and the possible host-guest interactions. Finally, the thermodynamic stability of the binary (cyclopentanemethanol + CH4) hydrate was relatively stable than that of the pure methane hydrate.

키워드

Clathrate hydrateCyclopentanemethanolGuest inclusionHydrogen bondingGuest interactionSELF-PRESERVATIONPHASE-EQUILIBRIAGAS HYDRATEMETHANEDEPENDENCESTORAGEGLYCOL
제목
Spectroscopic identifications of structure II hydrate with new large alcohol guest molecule (Cyclopentanemethanol)
저자
Park, Ki HunKim, Dong HyunCha, Minjun
DOI
10.1016/j.cplett.2021.138869
발행일
2021-09-16
유형
Article
저널명
Chemical Physics Letters
779